Beneficial Effect of a Pre-ceramic Polymer Coating on the Protection at 900 °C of a Commercial AISI 304 Stainless Steel

Abstract : An effective and low-cost method for applying polysilazane-based barrier coating on stainless steel is presented. A SiN (PHPS) precursor has been used for applications of polymeric and ceramic-like coating material. With precursor solution in dibutyl ether, AISI 304 stainless steel substrates were coated by means of a simple dip coating technique. After pyrolysis stage at 800 °C, the efficiency of the PHPS-based coating has been proved, and oxidation tests were done at 900 °C in air. By measuring the weight gain, and by using analytical techniques as in situ X-Ray Diffraction and Scanning Electron Microscopy, it has been shown that an amorphous silica layer formed from the initial PHPS-based coating and acts as a protective glass which provides complete separation of the AISI 304 steel surface from the oxidizing environment. This protective silica layer appears to be a very good diffusion barrier by preventing iron-containing oxide formation.
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Oxidation of Metals, Springer Verlag, 2017, 88 (1-2), pp.211-220. 〈10.1007/s11085-016-9705-1〉
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Frédéric Riffard, Eva Joannet, Henri Buscail, Raphaël Rolland, Sébastien Perrier. Beneficial Effect of a Pre-ceramic Polymer Coating on the Protection at 900 °C of a Commercial AISI 304 Stainless Steel. Oxidation of Metals, Springer Verlag, 2017, 88 (1-2), pp.211-220. 〈10.1007/s11085-016-9705-1〉. 〈hal-01659978〉

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